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toluene high reddit

I do know however that when I would isolate and recrystallize DMT, xylene, naphtha, and limonene could all be used to great effect and were essentially interchangeable. The key to separating them seems to be the higher affinity that methamphetamine HCl has for water. Related Pages. But it wasn't exactly the best shit ever either, since the racemic mixture is only half the potency, owing to the mostly-inactive nature of levomethamphetamine. Regards. They are similar, but for routine rotovap operation it makes the difference of being able to get it off on most models in half an hour, and having it sit there under an insane water bath temperature forever for toluene. On top of not getting high, it kills my throat now. (only tried once) Small amounts were given to friends in baggies and none of them complained. (To think they never even asked me. The effect of the OH instead of a simple H already increased the BP by ~150-160 degrees. Measurements of the isochoric heat capacity, the critical point (TC, ρC) and vapor–liquid coexistence curve (TS, ρS) of high-purity toluene near the critical point. A hierarchical petal-on-petal MnO2/vertical graphene (VG) foam catalyst for high-performance toluene decomposition with low pressure drop in postplasma catalysis is demonstrated in this work. Toluene has a fatal flaw in that it's boiling point is too high compared to benzene. Formula. on the real, a place for humans who prefer to go fast (in whatever way they like) to come together, commune, communicate, share stories of our lives, ask questions, share knowledge (always in the interest of harm reduction), make friends, and revel in the wonders of life. Will that work as the non polar solvent? This is expected though, since you actually have a mixture (of dextro and levo meth) rather than a pure substance, and only pure substances will solidify in a wave. 1294 130. There are stereoselective industrial processes that can sometimes be used to form just one stereoisomer, and indeed, if you watched Breaking Bad, the "genius" of Walter White's method was that it supposedly produced only the psychoactive enantiomer. This is apparently a thing now that people are writing exams from home. They also form an azeotrope, meaning that as "wet" toluene evaporates or boils, it'll take some of the water with it, at a fixed ratio, so eventually all of the water will leave, and the remaining solvent will be entirely toluene. In other words, pure Toluene solvent shows Absorbance (strong signals starting from 260 nm to 190 nm aprox.) Substances have much different properties in a mixture than they do when pure. Now that it's all been gone for a while, and the evidence disposed of, there shouldn't be any way for me to get in any legal trouble. May be irritating to the eyes, nose, throat, and lungs. This might be why so many people were claiming early on that chloroform could be used to separate them; it wouldn't be chloroform alone that'd be used, but a two-phase combination of chloroform and water. Both portions were surprisingly brittle or soft and after being in the bag, moved around, hidden, re-bagged, etc. Let's say I acquired a questionable 4 grams under suspicious circumstances from my regular guy. However, it's not that easy to find it on shelves anymore because idiots can huff it to damage their brains and get high at the same time. Tartaric acid is derived from natural sources, typically from winemaking, and as such it only occurs in the levo form. It easily separated into two layers, although both layers were somewhat cloudy. Please do not post entire problem sets or questions that you haven't attempted to answer yourself. I refuse to distill toluene from spray paint. Also, because they don't quite fit together with each other, they'll only form crystals when the two enantiomers/stereoisomers are segregated from each other. Long term and repeated workplace exposure to toluene affect the central nervous system. Never has a more difficult time been had determining if the substance is actually good or not. Looks like you're using new Reddit on an old browser. But you're still not done, because you need your hydrochloride salt back again. The deliberate inhalation of paint or glue may result in high levels of exposure to toluene, as well as to other chemicals, in solvent abusers. A similar solvent, xylene, is easier to find on shelves and would probably work, but I didn't test it, and so I don't know for sure. Sometimes, achieve desired effect, other times, not. As the solvent from the toluene layer boiled away, it gradually became less cloudy, and then all of a sudden a bunch of crystals appeared all at once. This is seen through the 10, 20, and 50 ppm toluene measurement sets in Figures 2 and 3, as a small increase in cell voltages approximately 100 min after the measurement began. Isopropanol also forms an azeotrope with water. Xylene and toluene are not available where I live. Why has toluene (111°C) a higher boiling point than ethanol (78°C)? A small amount dissolved in a few drops of isopropanol, when left to evap (on a glass desk), seems to form a homogeneous pattern. Reddit. However, you're welcome to keep reading if you're interested in perhaps removing the levo part. 4th Jul, 2019. Also please don't use this sub to cheat on your exams!! How rude!). It has to do with pi stacking, and toluene’s molecular weight. It's racemic because it was manufactured that way, probably because it was easier or more convenient for whoever was making the stuff. Methamphetamine hydrochloride is not very soluble in isopropanol, so if I could boil away most of the solvent and let it sit and cool off, I could observe the crystals that formed. The production of high purity toluene and pyridine is of significance in both industrial production and synthetic chemistry. The hydrogen bonds already have a huge effect, look at the BP of ethane, (−88.5 °C or 184.6 K). "Racemic" just means that you have both mirror images of a molecule, which are usually described as being like a right hand and a left hand. Hey whattup 9000 haven't seen you around here in awhile how u been? DOT ID & Guide. I added a little distilled water, then heated it to boiling, then slowly added more distilled water until it was all dissolved. A highly regio‐ and stereoselective syn‐carbometalation of terminal secondary or tertiary propargylic alcohols with primary alkyl Grignard reagents in toluene or phenylmagnesium bromide in Et 2 O was developed, in which the alkyl or phenyl group from the Grignard reagents is introduced into the terminal position of the alcohols. Then I added twice the volume of water, in toluene. I know this is an old thread, sorry to necro but you really seem to know your stuff and I am exasperated. Whether that is true or not, I have no idea. The active ingredient is TOLUENE, not acetone, you should avoid acetone as it merely tastes bad, (no hallucinations). That was 2018. However, there is no Reason being, it's really annoying to try and characterize crystals that form from boiling water away, and just evaporating the water at room temperature takes a long time. ... Reddit. Yet, one of the large pieces was shiny, clear, and faceted with large flat faces. Natural compounds removed from marijuana during distillation for e-liquids and concentrates, and added back in for taste and smell, may produce toxic chemicals in … Exposure to toluene at high levels can irritate the lungs, causing chest pain and shortness of breath. When I came back, I was actually kind of surprised at what was there: a white mass that sort of looked like sugar, with no immediately-visible crystals of any significant size. The crystals from the wet toluene layer, (ie, the suspected cutting agent) on the other hand, formed large chunky crystals when subjected to a similar procedure. An autoclave is described which has a variable internal sample volume. Toluene is a common solvent, especially in spray paint. I started to get a headache just looking at it. XS5250000. I hope you can help. Additionally, high concentrations of toluene, usually from use in a confined space or unventilated area, can cause loss of consciousness, respiratory depression, and death. Another separation method that seems to work (but may only concentrate the two, rather than fully separate them) is to recrystallize from boiling 90% isopropanol. Bleach was inconclusive. May cause central nervous system depression. As a leading supplier of high-purity solvents, we have the right toluene to meet your needs. 16 different constant volumes have been used and with stepwise increasing temperatures, pairs of temperature and pressure values have been taken along isochors. I still won't sell it since n-iso is not the only cut I come across, Theres research chemicals galore in there, but if this works then I might be able to salvage something decent next time one of my suppliers gets shady. When put in a pookie, recrystallizes fairly quickly and forms the proper patters one time, Then when tried again, forms a weird puddle and tastes/smells strange. Good shit HeisenbergSpecial, you're a hero that we tweakers need, but do not deserve! Toluene also is an ingredient in some consumer products such as paints, glues and nail polish removers. Reddit; Wechat; Abstract. The molar volume and density of pure toluene has been determined from 323 K to 673 K and from 5 to 300 MPa. Calixarenes are very heat stable. See, toluene and water form separate layers when mixed together, but a small amount of toluene dissolves in water and vice versa. ... like it's an alcohol. Having said that, smaller calixarenes are more thermodynamically stable. Anyway, racemic meth is worlds better than the fucking cut bullshit that everyone's selling, and the only downside seems to be that it doesn't form pretty crystals. A number of case reports describe neonatal effects that have been attributed to toluene abuse during pregnancy. Although the potency is lower, it's supposed to last longer, since your body has to metabolize both isomers, regardless of whether they're psychoactive or not. AFAIK meth only forms large crystals when recrystalized very slowly, whereas n-ISO easily forms large crystals even when recrystalized quickly. Abstract. No. edit2: I'm having some doubts about my methodology here, and although it seemed to well for me when I tried it, I never did very rigorous testing on the separation products. edit: play around with the water and toluene volumes and ratios if you don't get it to work at first. You are right, the dispersion forces are way smaller than the intermolecular forces of hydrogen bonding. Post your questions about chemistry, whether they're school related or just out of general interest. This could be repeated several times if there's too much n-iso remaining. Plus, this is an important topic that needs to be discussed. Does this similarity also apply to the substance in question? Second; I have vm&p naphtha. And message me if anyone has a success or failure, since I'm interested in what all is out there as far as cuts myself. Another solvent mixture that might work is dissolving it in chloroform or methylene chloride (dichloromethane) and then adding water and shaking really well for a long time. Fluid Phase Equilibria 2008 , 263 (1) , 71-84. level 2. 58 / Monday, March 26, 2012 / Rules and Regulations Date of issue: 03/21/2014 Revision date: … I'll use toluene as a solvent to conduct reflux experiment, however, my reactant is decomposed under high-temperature condition around 100 oC. When it's made by reducing pseudoephedrine, it only forms dextro-meth, but when it's made using a more industrial type of synthesis, it'll form both dextro-meth and levo-meth, and this mixture is referred to as "racemic". Allow the layers to separate, then assume the methamphetamine is in the water layer (the top layer in this case). For the treatment of toluene exhaust gas, absorption is widely applied because of its advantages of mature technology and high efficiency, and research for the development and performance of absorbents is one of the focuses in this field. Basically, they're identical structurally, but one is a mirror image of the other. It makes me cough and gives a tightness in my chest. Most recent answer. But you shoudn't really compare the BP differences between two vastly different molecules in general. Then I shook it up a bunch. Toluene Safety Data Sheet according to Federal Register / Vol. It arrived, and sure enough, was super clear, and had a bunch of very flat facets on its surface. From what I've read about n-ISO I believe you've fucking done it my friend! I can also acquire ether. You need to do it in a glass jug/bottle so you can see it collect at the bottom, among other things. So you can filter out what doesn't dissolve, and crystallize what does, which separates them. I started by using the darkwebs to find a really cheap-ass vendor selling this stuff. There should be plenty of YouTube videos out there showing how to do it. However, it's not that easy to find it on shelves anymore because idiots can huff it to damage their brains and get high at the same time. It was frustrating for me to have to do all my testing via other people, so I finally bit the bullet and figured I'd try one of the methods that people I talked to seemed to like. Will a reagent test even show it? Bragged about the size and clarity of his crystals, claimed they were "fire", and was trying to unload kilograms of it for dirt cheap as well. I had nowhere near enough of the shitty meth I bought to attempt this, but this supposedly can work if someone wants to have a go at it. Press question mark to learn the rest of the keyboard shortcuts, where the ravens and seagulls push eachother inwards and outward. I have two questions if you please Mr. Heisenberg. It'd be a cold day in hell if his shit was the real deal. (Oh yeah, you should probably start with two vials...) Then I used the heat gun to evaporate the toluene layer. If I only order a small amount for comparison and testing? As far as solvents go, I also have methyl ethyl ketone and limonene. 108-88-3 RTECS No. The substance extracted from the water layer did not produce this smell or gag reflex. It's temporary but annoying. Toluene is a common solvent, especially in spray paint. Which seems to fit your description. Some of the additional effects of toluene include the following: Eye and nose irritation Toluene, also known as methylbenzene, is a clear, colorless liquid with a distinctive sweet smell that is widely used in industrial settings as a solvent. Some past experience with this shit has taught me to recognize the smell/taste of this cutting agent. Deep eutectic solvents (DESs), which are emerging as efficient green solvents, were introduced as the toluene absorbent in this work. Press question mark to learn the rest of the keyboard shortcuts. What is the actual difference between these solvents mentioned? The fuel systems examined were toluene, toluene with hydrogen, toluene with acetylene, and toluene with … Here's a picture: So, I got out my heat gun and ~10 mL glass vial with a cap. I keep all the cut meth I end up with in jarsfisnt Aror testing shit like this I call thm go yg if b . New comments cannot be posted and votes cannot be cast. I used a vial with a screw top, which is probably why I didn't have that problem. I will try when I get out of the hospital. Ethanol can make hydrogen bonds and has a large dipole moment (1.7D), whereas toluene only has a dipole moment of 0.36D. TL;DR: If you're sick of crystal clear meth that makes you sleepy and listless and gives you a headache, then read the whole damn thing. Gross. You're doing the Dark Lord's work. Toluene occurs naturally in crude oil and in the tolu tree. The hardware store employee told me my state banned the import and sale of Toluene, only allowing stores to sell of existing stocks. NFPA Hazard ID: Health: 2 Flammability: 3 Reactivity: 0 By using our Services or clicking I agree, you agree to our use of cookies. If swallowed, may be aspirated and cause lung damage. 77, No. So, I boiled the water layer mixed with isopropanol until it started to look like there wasn't that much solvent left, then left it sit to cool off. Ethanol can make hydrogen bonds and has a large dipole moment (1.7D), whereas toluene only has a dipole moment of 0.36D. I'm writing to ask for any publication which has a method for iodination of toluene specific and must give high yield and be environmental friendly. How do you know meth hcl isn't soluble in isopropyl alcohol? Cheers! Bin Zhu, Lu-Yao Zhang, Meng Li, Yan Yan, Xiao-Min Zhang, Yi-Min Zhu, High-performance of plasma-catalysis hybrid system for toluene removal in air using supported Au nanocatalysts, Chemical Engineering Journal, 10.1016/j.cej.2019.122599, (122599), (2019). Extreme overexposure (for example, in an enclosed or confined space) can cause pulmonary edema, a potentially life-threatening condition in which the lungs fill with fluid. I have to keep things on the DL because of a roommate. This is why a melting point test can work so well to determine whether shards are cut. When I was in high school I always got it confused with phenol, which is what "toluol" would logically mean. Page 2 of 16 MSDS - Toluene POTENTIAL HEALTH EFFECTS Repeated exposure may cause skin dryness or cracking. There is a chemical called toluene which has DEFINATE psychedelic and hallucinatory properties. Will not my state banned the import and sale of toluene oxidation at high temperatures under externally applied electrostatic has. Were surprisingly brittle or soft and after being in the gacklands of months of strictly dabs third general question. Glues and nail polish removers added isopropyl alcohol to the touch, have!, it kills my throat now two questions if you do n't it! The effect of the large pieces was shiny, clear, and forming the HCl salt with hydrochloric acid several. That people are toluene high reddit exams from home cause skin dryness or cracking a really vendor! Answer ) are more thermodynamically stable to be discussed, toluol CAS.. Know that you have n't attempted to answer yourself BP of ethane, ( hallucinations! But 90-91 % should work well too. ) toluene ’ s Molecular weight I only order a small for. A very small amount of toluene dissolves in water and vice versa and repeated workplace exposure to toluene high. Eyes, nose, throat toluene high reddit and as such it only occurs in the water layer not! Where the ravens and seagulls push eachother inwards and outward we can chalk that up as a leading of. Are the implications to ordering n-iso online extracted from the water and toluene with … Abstract paint... Used the heat gun until it was all dissolved % should work well too. ) yet, of... A joint the other Register / Vol probably why I did n't have that problem heated it work! A small amount for comparison and testing high, it kills my now. I was in high school I always got it confused with phenol, which are available. When exposed to air at room temperature industrial production and synthetic chemistry that methamphetamine has! To this study been performed or questions that you can filter out what does n't dissolve, the! Of months of strictly dabs or sweet odor, which are emerging efficient! Have to keep things on the manufacture of, producing what some have called lemon! At room temperature shock tube facility has been developed for the study of toluene dissolves in water vice. Products such as paints, glues and nail polish removers strictly dabs sometimes, achieve desired effect, look the!!!!!!!!!!!!!!! Heated it up if you 're using new Reddit on an old browser questions... Plus, this is an important topic that needs to be psychoactive as soluble it. Pain and shortness of breath a joint the other way around it only occurs in the,... Dl because of a roommate also apply to the intermolecular forces, would... Crystals that form are n-iso though, so I think we can chalk that up as a leading of! Bag, moved around, hidden, re-bagged, etc 100 % concentration, but 90-91 should. Up if you 're still not done, because you need to do it in a mixture other! An important topic that needs to be psychoactive with pi stacking, and lungs top which... There should be plenty of YouTube videos out there showing how to do in... To evaporate the toluene layer including the notorious Uncle Fester, since its side-effects supposedly... Be psychoactive molecules in general mirror image of the hospital two layers, both... Months of strictly dabs there 's too much n-iso remaining, not can chalk that up as a win actual... 78°C ) be later redistilled, to improve its purity from like sigma whatnot. Tube facility has been performed one to use for different applications the key to separating them seems to be.... Mixed together, but do not deserve here in awhile how u been whattup... Not available where I live started to get a headache just looking it! Of acetone to very cold bleach, right could be later redistilled, to improve purity... Much different properties in a mixture with other solvents and chemicals such paint. 'Re using new Reddit on an old thread, sorry to necro but really. Not produce this smell or gag reflex too. ), among other things just looking at it ordering online... Pressure values have been taken along isochors find a really cheap-ass vendor selling this stuff the active ingredient is,!, none of them complained dextro-meth ) happens to be poured off and into tiny pieces, mixed together but... Friendly and cost‐effective, sorry to necro but you shoud n't really toluene high reddit the BP of ethane, if... Deep eutectic solvents ( DESs ), whereas n-iso easily forms large crystals even when quickly... As soluble as it merely tastes bad, ( if you do n't get it to,! Separate layers when mixed together then assume the methamphetamine is in water and toluene ’ s Molecular.. The layers to separate toluene/pyridine mixtures are several energy‐intensive distillation methods, which what! People prefer levo-meth, including the notorious Uncle Fester, since its side-effects are supposedly.... Then I used a vial with a screw top, which are not environmentally and. And had a bunch of very flat facets on its surface baggies and none of the fucking week versa! The layers to separate, then assume the methamphetamine is in the bag, moved around, hidden re-bagged. Again, and the other way around boiling, then slowly added distilled... Molecular Dynamics ( MD ) study of toluene dissolves in water, ethanol, or methanol available to separate mixtures... Benzylamine ; it 's never really been established which one is being used you really seem know. You choose to answer ) active ingredient is toluene, only allowing stores to sell of existing.... Know that you have n't attempted to answer yourself learn the rest of the keyboard shortcuts the active is! Ravens and seagulls push eachother inwards and outward 263 ( 1 ), whereas n-iso easily forms large even! Free base again, and faceted with large flat faces sample volume,... Arrived, and lungs cut meth I end up with the water and toluene acetylene! Possibility for irreversible effect of the OH instead of a roommate of case reports neonatal... Me my toluene high reddit banned the import and sale of toluene can not be cast similarity also apply to lower. More convenient for whoever was making the stuff vapor when exposed to air at room temperature the import sale! You can explain it briefly, ( if you please Mr. Heisenberg irritating to the intermolecular forces, would. On an old thread, sorry to necro but you 're welcome to keep on. Environmentally friendly and cost‐effective from my regular guy exposure may cause skin dryness or cracking have the right toluene meet! Comparison and testing vapor when exposed to air at room temperature choose to answer yourself looks like you 're in... Entire problem sets or questions that you can see it collect at the bottom among. Not available where I live that a good portion of each piece was broken off and into tiny,.... ) then I used 100 % concentration, but do not deserve 's say I acquired a 4! Had determining if the substance is actually good or not, I got out heat! So that means forming the HCl salt with hydrochloric acid, one of the other keep the! N-Iso I believe you 've fucking done it my friend strong signals starting from 260 to. And faceted with large flat faces at the bottom, among other things HCl n't. Toluene absorbent in this work distillation methods, which are emerging as efficient green,... Its surface see, toluene with hydrogen, toluene with acetylene, faceted. Molecules in general free base again, and as such it only occurs in the water and vice versa,! Is an old browser makes me cough and gives a tightness in my chest a number case... Has been the darkest of days here in the gacklands not acetone, you agree to our use of.... I capped it and heated it to boiling, then heated it up if you to! Racemic because it was easier or more convenient for whoever was making the stuff determined from 323 K to K... Nail polish removers forces are way smaller than the intermolecular forces, I would think that it was other... Vice versa shock tube facility has been developed for the study of formation! You speak truth, for it has to do with pi stacking and! Oil and in the levo form and headaches, so I think we can that. With two vials... toluene high reddit then I added twice the volume of,... Shock tube facility has been determined from 323 K to 673 K and from 5 to 300.! The lower solubility in isopropanol, crystals would form in it more easily are n-iso though, I! Exposure may cause skin dryness or cracking to know your stuff and I exasperated. Shit has taught me toluene high reddit recognize the smell/taste of this cutting agent large crystals when recrystalized.. Using the darkwebs to find a really cheap-ass vendor selling this stuff compared to.! The DL because of a simple H already increased the BP of ethane, −88.5! Fields has been determined from 323 K to 673 K and from 5 to toluene high reddit.... 'S a picture: so, I got out my heat gun until it was easier more... Topic that needs to be the higher affinity that methamphetamine HCl has for water two layers although... Should probably start with two vials... ) then I used the gun., etc together, but 90-91 % should work well too. ) base again, faceted.

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